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Q.

The strength of an aqueous NaOH solution is most accurately determined by titrating: (Note: consider that an appropriate indicator is used) 
 

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a

Aq. NaOH in a burette and aq. Oxalic acid in a conical flask 
 

b

Aq. NaOH in a volumetric flask and conc. H2SO4 in a conical flask 
 

c

Aq. NaOH in a pipette and aqueous oxalic acid in a burette 
 

d

Aq. NaOH in a burette and conc. H2SO4 in a conical flask 
 

answer is A.

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Detailed Solution

The strength of NaOH measured by titrating against oxalic by taking NaOH in the burette and oxalic acid in the conical flask. We always prepared fresh oxalic acid solution because it is a primary standard and NaOH secondary.

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The strength of an aqueous NaOH solution is most accurately determined by titrating: (Note: consider that an appropriate indicator is used)